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    XING Xin, LI Xiao-dong, GUO Ai-qing, CAO Feng, WANG Jun. Preparation of Polychloromethylsilane from Chlorination of Polymethylsilane[J]. Journal of Functional Polymers, 2004, 17(2): 181-184.
    Citation: XING Xin, LI Xiao-dong, GUO Ai-qing, CAO Feng, WANG Jun. Preparation of Polychloromethylsilane from Chlorination of Polymethylsilane[J]. Journal of Functional Polymers, 2004, 17(2): 181-184.
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    Preparation of Polychloromethylsilane from Chlorination of Polymethylsilane

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    • Polychloromethylsilane (PCMS) was synthesized by chlorination of polymethylsilane (PMS) at room temperature using CCI_4 as chlorinsting agent. Its structure was recognized by ~1H-NMR and ~(29)Si CP MAS-NMR. The effects of reaction time and the molecular s
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