Rink酸树脂—4—（2′,4′—二甲氧基苯羟甲基）苯氧甲基聚苯乙烯的合成

范云鸽, 史作清. Rink酸树脂—4—（2′,4′—二甲氧基苯羟甲基）苯氧甲基聚苯乙烯的合成[J]. 功能高分子学报, 2000, 13(4): 437-439.

引用本文:

范云鸽, 史作清. Rink酸树脂—4—（2′,4′—二甲氧基苯羟甲基）苯氧甲基聚苯乙烯的合成[J]. 功能高分子学报, 2000, 13(4): 437-439.

摘要: 加入ＫＩ可使Ｌｉｎｋｅｒ（Ｉ）与氯甲基聚苯乙烯的反应时间大大缩短；在用ＮａＢＨ４还原时加入金属卤化物增强其还原能力，制备出Ｒｉｎｋ酸树脂。

Abstract: Ketone linker(I) was coupled to chloromethylated polystyrene via the addition of K 2CO 3 instead of the expensive Cs 2CO 3, and the reaction time was reduced greatly by addition of a little KI; ketone resin(II) was reduced by NaBH 4 in THF adding AlC

/