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    黄昌国, 万小龙. 原子转移自由基聚合制备聚酯二元醇接枝聚苯乙烯[J]. 功能高分子学报, 2000, 13(2): 169-172.
    引用本文: 黄昌国, 万小龙. 原子转移自由基聚合制备聚酯二元醇接枝聚苯乙烯[J]. 功能高分子学报, 2000, 13(2): 169-172.
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    Sythesis of Polyester Polyol-g-Polystyrene by Atom Transfer Radical Polymerization[J]. Journal of Functional Polymers, 2000, 13(2): 169-172.
    Citation: Sythesis of Polyester Polyol-g-Polystyrene by Atom Transfer Radical Polymerization[J]. Journal of Functional Polymers, 2000, 13(2): 169-172.
    shu

    原子转移自由基聚合制备聚酯二元醇接枝聚苯乙烯

    Sythesis of Polyester Polyol-g-Polystyrene by Atom Transfer Radical Polymerization

      摘要
    • 摘要: 聚酯二元醇经氯甲基化制备了聚酯二元醇大分子引发剂，通过原子转移自由基聚合技术，合成了聚酯二元醇－ｇ－聚苯乙烯接枝聚合物。用＾１Ｈ－ＮＭＲ、ＦＴ－ＩＲ和ＧＰＣ表征了接枝聚合物，结果表明分子量与转化率呈线性关系，且分子量分布较窄，接枝聚合反应是一个可控过程。

       

      Abstract: Chloromethylated polyester polyol, the macroinitiator for atom transfer radical polymerization (ATRP), was prepared by chloromethlating the aromatic rings of polyester's backbone. Polyester polyol-g-polystyrene was synthesized by CuCl-catalyzed ATRP of st

       

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